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Determination of impurities in fixed vegetable oils

Abstract

The review contains summary information about possible impurities, determination of which is described by draft monograph «fixed vegetable oils» and state standards of Russian Federation. The review briefly describes methods for determination of soaps, unsaponifiable components, residual solvents, volatile compounds, foreign fatty oils, aldehydes, moisture, proteins, paraffin, wax, tar and mineral oils, heavy metals, phosphorus-containing substances, cyanides and hydrogen cyanides.

About the Authors

A. M. Kalinin
Federal State Budgetary Institution «Scientific Centre for Expert Evaluation of Medicinal Products» of the Ministry of Health of the Russian Federation
Russian Federation


N. P. Antonova
Federal State Budgetary Institution «Scientific Centre for Expert Evaluation of Medicinal Products» of the Ministry of Health of the Russian Federation
Russian Federation


S. S. Prokhvatilova
Federal State Budgetary Institution «Scientific Centre for Expert Evaluation of Medicinal Products» of the Ministry of Health of the Russian Federation
Russian Federation


E. P. Shefer
Federal State Budgetary Institution «Scientific Centre for Expert Evaluation of Medicinal Products» of the Ministry of Health of the Russian Federation
Russian Federation


References

1. Fixed vegetable oils. Draft monograph [Internet]. 2015 [cited 2015 Aug 10]. Available from: http://www.rosminzdrav.ru/ministry/61/11/materialy-po-deyatelnosti-deparatamenta/stranitsa-856/spisok-obschih-farmakopeynyh-statey (in Russian).

2. Tyutyunnikov BN, Buhshta ZI, Gladkiy FF et al. Chemistry of fats. 3rd ed. Moscow: Kolos; 1992 (in Russian).

3. The State Pharmacopoeia of USSR. 10th ed. Moscow: Meditsina; 1968 (in Russian).

4. The State Pharmacopoeia of Russian Federation. 12th ed. V. 1. Moscow: Federal State Budgetary Institution «Scientific Centre for Expert Evaluation of Medicinal Products» of the Ministry of Health of the Russian Federation; 2007 (in Russian).

5. O’Brien RD. Fats and oils: formulating and processing for applications. 2nd ed. Boca Raton: CRC Press LLC; 2004.

6. State Standard 5480-59. Vegetable oils and natural fatty acids. Methods for determination of soaps (in Russian).

7. American oil and chemists’ society. The official methods and recommended practices of the American oil chemists’ society. 4th ed. Champaign, IL: AOCS Press; 1994.

8. State Standard 31753-2012. Vegetable oils. Methods for determination of phosphorus-containing substances. Moscow: Standartinfrom; 2014 (in Russian).

9. The State Pharmacopoeia of USSR. 11th ed. V. 1. Moscow: Meditsina; 1987 (in Russian).

10. State Standard 31933-2012. Vegetable oils. Methods for acid number determination. Moscow: Standartinfrom; 2014 (in Russian).

11. State Standard 30418-96. Vegetable oils. Method for determination of fatty acid composition (in Russian).

12. European Pharmacopoeia. 8th ed. [Internet]. 2015 [cited 2015 Aug 31]. Available from: http://online.edqm.eu/entry.htm.

13. Dieffenbacher A, Pocklington WD. Standard methods for the analysis of oils, fats and derivatives. Oxford: Blackwell Science; 1992.


Review

For citations:


Kalinin A.M., Antonova N.P., Prokhvatilova S.S., Shefer E.P. Determination of impurities in fixed vegetable oils. The Bulletin of the Scientific Centre for Expert Evaluation of Medicinal Products. 2015;(4):51-53. (In Russ.)

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ISSN 3034-3062 (Print)
ISSN 3034-3453 (Online)